Comparative Synthesis of Silver Nanoparticles: Evaluation of Chemical Reduction Procedures, AFM and DLS Size Analysis

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dc.authoridCHICEA, Dan/0000-0001-8074-9107
dc.authoridOzkendir, Osman Murat/0000-0002-0810-9938
dc.authoridNicolae-Maranciuc, Alexandra/0000-0003-0742-241X
dc.contributor.authorChicea, Dan
dc.contributor.authorNicolae-Maranciuc, Alexandra
dc.contributor.authorDoroshkevich, Aleksandr S.
dc.contributor.authorChicea, Liana Maria
dc.contributor.authorOzkendir, Osman Murat
dc.date.accessioned2025-03-17T12:25:15Z
dc.date.available2025-03-17T12:25:15Z
dc.date.issued2023
dc.departmentTarsus Üniversitesi
dc.description.abstractThe size of silver nanoparticles plays a crucial role in their ultimate application in the medical and industrial fields, as their efficacy is enhanced by decreasing dimensions. This study presents two chemical synthesis procedures for obtaining silver particles and compares the results to a commercially available Ag-based product. The first procedure involves laboratory-based chemical reduction using D-glucose (C6H12O6) and NaOH as reducing agents, while the second approach utilizes trisodium citrate dehydrate (C6H5Na3O7 & BULL;2H(2)O, TSC). The Ag nanoparticle suspensions were examined using FT-IR and UV-VIS spectroscopy, which indicated the formation of Ag particles. The dimensional properties were investigated using Atomic Force Microscopy (AFM) and confirmed by Dynamic Light Scattering (DLS). The results showed particle size from microparticles to nanoparticles, with a particle size of approximately 60 nm observed for the laboratory-based TSC synthesis approach.
dc.description.sponsorshipLucian Blaga University of Sibiu amp; Hasso Plattner Foundation [LBUS-IRG-2020-06, LBUS-IRG-2022-08]
dc.description.sponsorshipThis research was financed by Lucian Blaga University of Sibiu & Hasso Plattner Foundation research grants LBUS-IRG-2020-06 and through the research grant LBUS-IRG-2022-08.
dc.identifier.doi10.3390/ma16155244
dc.identifier.issn1996-1944
dc.identifier.issue15
dc.identifier.pmid37569948
dc.identifier.scopus2-s2.0-85167777714
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.3390/ma16155244
dc.identifier.urihttps://hdl.handle.net/20.500.13099/1578
dc.identifier.volume16
dc.identifier.wosWOS:001045682600001
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoen
dc.publisherMdpi
dc.relation.ispartofMaterials
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_WOS_20250316
dc.subjectsilver nanoparticles
dc.subjectchemical synthesis
dc.subjectparticle sizing
dc.subjectDLS measurements
dc.subjectAFM analysis
dc.subjectlocalized surface plasmon resonance (LSPR)
dc.titleComparative Synthesis of Silver Nanoparticles: Evaluation of Chemical Reduction Procedures, AFM and DLS Size Analysis
dc.typeArticle

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