Microwave-assisted high-pressure CO2-water extraction of pectin from baobab fruit ( Adansonia digitata L): Effects on yield and characterization

dc.contributor.authorDemir, Aysel Elik
dc.contributor.authorMendy, Mandalena
dc.date.accessioned2025-03-17T12:27:02Z
dc.date.available2025-03-17T12:27:02Z
dc.date.issued2024
dc.departmentTarsus Üniversitesi
dc.description.abstractPectin, extensively used in the industry for various purposes, is abundantly present in baobab fruit (Adansonia Digitata L.). This study aimed to investigate the microwave-assisted high-pressure CO2-water (MCAPE) technique, an innovative and environmentally friendly method, to extract this valuable compound. This approach utilizes the combination of microwave technology, high pressure, CO2, and water (instead of organic solvent), achieving an effective and rapid process to produce hazard-free pectin. The optimization of the MCAPE system was carried out using the Box-Behnken design of the response surface methodology. Extraction time (2-7 min), temperature (60-80 degrees C) and pulp to water ratio (1:10-1:20 g/ml) were selected as the process variables. The optimum extraction conditions to obtain the highest extraction yield (32.42 %) were determined as a temperature of 73 degrees C, extraction time of 4.3 min, and pulp to water ratio of 1:18 g/mL. The pectin obtained by the MCAPE technique at optimum conditions was compared to the pectin obtained by the conventional pectin extraction in terms of pectin yield, moisture content, ash content, protein content, degree of esterification, galacturonic acid content, total phenolic content, antioxidant activity, and structural characterization. Overall, the results revealed that the MCAPE was a novel, fast, effective, and green technique for extracting the pectin from food materials.
dc.description.sponsorshipErasmus + Programme
dc.description.sponsorshipThe authors thank to Prof. Dr. Fahrettin Gogues , and Assoc. Prof. Dr. Derya Kocak Yan & imath;k for providing laboratory support. Additionally, Mandalena Mendy thanks for a scholarship within the Erasmus + Programme.
dc.identifier.doi10.1016/j.microc.2024.112250
dc.identifier.issn0026-265X
dc.identifier.issn1095-9149
dc.identifier.scopus2-s2.0-85209899856
dc.identifier.scopusqualityQ1
dc.identifier.urihttps://doi.org/10.1016/j.microc.2024.112250
dc.identifier.urihttps://hdl.handle.net/20.500.13099/2017
dc.identifier.volume207
dc.identifier.wosWOS:001366991400001
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofMicrochemical Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250316
dc.subjectPectin
dc.subjectCharacterization
dc.subjectExtraction
dc.subjectMicrowave
dc.subjectCO2
dc.titleMicrowave-assisted high-pressure CO2-water extraction of pectin from baobab fruit ( Adansonia digitata L): Effects on yield and characterization
dc.typeArticle

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