Insights into the promising heterogeneous catalysis of eco-friendly synthesized spinel CuFe2O4 nanoparticles for Biginelli reaction

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dc.authoridA. Ahire, Dr. Satish/0000-0002-6333-3553
dc.contributor.authorSanap, Dnyaneshwar
dc.contributor.authorAvhad, Lata
dc.contributor.authorAhire, Satish
dc.contributor.authorMirzaei, Mahmoud
dc.contributor.authorKumar, Deepak
dc.contributor.authorGhotekar, Suresh
dc.contributor.authorGaikwad, Nitin D.
dc.date.accessioned2025-03-17T12:27:35Z
dc.date.available2025-03-17T12:27:35Z
dc.date.issued2024
dc.departmentTarsus Üniversitesi
dc.description.abstractSpinel copper ferrite magnetic nanoparticles (CuFe2O4 MNPs) are one of the prominent spinel ferrites due to their magnetic properties. As a result of the current investigation, the magnetic spinel copper ferrite nanoparticles (CuFe2O4 MNPs) were successfully fabricated via a green synthesis approach using freshly prepared Yogurt of cow milk as a capping agent by sol-gel auto-combustion route and its catalytic effect towards synthesizing ethyl 1,2,3,4-tetrahydro-2-oxo-4-aryl pyrimidine-5-carboxylate (DHPMs) scaffold was explored. Further, the phase formation, crystallinity, particle size, grain morphology, and the property of magnetism of bio-fabricated spinel CuFe2O4 NPs were explored by XRD, FESEM, EDX, FTIR, UVDRS, and VSM analysis. Furthermore, one-pot synthesis of DHPMs scaffold via multicomponent (MCR) Biginelli reaction was examined using biosynthesized spinel CuFe2O4 magnetic heterogeneous catalyst (C1 and C2 nanocrystalline phase). To achieve the high yields (90-98%) of DHPMs scaffold synthesis with an extensive range of aromatic carbaldehyde using minimum loading of heterogeneous catalysts within minimum reaction time and easy catalyst recovery by a peripheral magnet were examined. Therefore, this protocol presents an extensive scope for Biginelli reaction using magnetically separable heterogeneous catalyst synthesis via a green approach.
dc.identifier.doi10.1007/s11164-024-05322-5
dc.identifier.endpage3711
dc.identifier.issn0922-6168
dc.identifier.issn1568-5675
dc.identifier.issue8
dc.identifier.scopus2-s2.0-85196042627
dc.identifier.scopusqualityQ2
dc.identifier.startpage3687
dc.identifier.urihttps://doi.org/10.1007/s11164-024-05322-5
dc.identifier.urihttps://hdl.handle.net/20.500.13099/2326
dc.identifier.volume50
dc.identifier.wosWOS:001248445700002
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofResearch On Chemical Intermediates
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250316
dc.subjectGreen synthesis
dc.subjectCuFe2O4 NPs
dc.subjectHeterogeneous nanocatalysis
dc.subjectMagnetically retrievable catalyst
dc.titleInsights into the promising heterogeneous catalysis of eco-friendly synthesized spinel CuFe2O4 nanoparticles for Biginelli reaction
dc.typeArticle

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